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How to boil 99% IPA Options
 
w0mbat
#1 Posted : 12/20/2009 11:30:00 PM
Can anyone think of a way to do this safely, assuming one did not have a hot plate? Maybe a microwave? SWIM was thinking of using a boiling water bath, but does not want to make his 99% IPA pick up moisture from the boiling water.
benzyme wrote:

i'm tellin ya, one day i'll interface a mass spec and uv-vis spectrophotometer to a modular synthesizer

 
Madcap
#2 Posted : 12/21/2009 12:15:47 AM
w0mbat wrote:
Can anyone think of a way to do this safely, assuming one did not have a hot plate? Maybe a microwave? SWIM was thinking of using a boiling water bath, but does not want to make his 99% IPA pick up moisture from the boiling water.

Stovetop in glass casserole dish. Assuming you have electric stove Smile
All posts written by Madcap should be regarded as fiction.
 
Jorkest
Moderator | Skills: Extraction Troubleshooting, (S)elf ProgrammingChemical expert | Skills: Extraction Troubleshooting, (S)elf Programming
#3 Posted : 12/21/2009 12:18:37 AM
you do not want to put ISO in the microwave..that sounds like a really bad idea


i dont think there are many safe ways to BOIL IPA...just remember..boiling solvents = dangerous no matter how you do it...BE VERY CAREFUL
it's a sound
 
1992
#4 Posted : 12/21/2009 12:23:34 AM
put it under a vacuum brotherman
 
w0mbat
#5 Posted : 12/21/2009 12:50:54 AM
1992 wrote:
put it under a vacuum brotherman

I think it needs to be boiled with heat to make "stuff" more soluble in it.

No electric stove unfortunately, maybe I should get one of those cheap plugin ones from walmart? Or just throw down the extra $ for a hotplate?
benzyme wrote:

i'm tellin ya, one day i'll interface a mass spec and uv-vis spectrophotometer to a modular synthesizer

 
1992
#6 Posted : 12/21/2009 1:00:37 AM
^ if you change le pressure you can get a lower boiling point dudo. Easier more ghetto method would to be put it in a plastic bag in throw it in some boiling or near boiling water. The microwave idea is not a good one
 
Jorkest
Moderator | Skills: Extraction Troubleshooting, (S)elf ProgrammingChemical expert | Skills: Extraction Troubleshooting, (S)elf Programming
#7 Posted : 12/21/2009 1:57:03 AM
just got the cheap electric hotplate from walmart...bought one for 10 bucks..its awesome...then get an IR thermometer
it's a sound
 
w0mbat
#8 Posted : 12/21/2009 3:41:28 AM
Would a glass mercury thermometer work as well, if I bring the temp up really slowly?
benzyme wrote:

i'm tellin ya, one day i'll interface a mass spec and uv-vis spectrophotometer to a modular synthesizer

 
Jorkest
Moderator | Skills: Extraction Troubleshooting, (S)elf ProgrammingChemical expert | Skills: Extraction Troubleshooting, (S)elf Programming
#9 Posted : 12/21/2009 5:09:59 AM
i dont think that would give you a very accurate reading
it's a sound
 
Jorkest
Moderator | Skills: Extraction Troubleshooting, (S)elf ProgrammingChemical expert | Skills: Extraction Troubleshooting, (S)elf Programming
#10 Posted : 12/21/2009 6:03:10 AM
the safest way to boil IPA is OUTSIDE with an electric hotplate...still be SUPER careful though..because any spark could cause some sort of fire...also..be very careful because its HOT....but do it outside..away from prying eyes and noses..and do it as fast and carefully as you can...
it's a sound
 
 
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